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Fristam FCM eliminates ingredient separation – Emulsifying cedar oil into insecticide formulation

High performance homogenisation of eco-friendly insecticides.

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Introduction to the application and industry overview

The production of environmentally friendly insecticides requires stable emulsification, uniform active ingredient distribution, and consistent product quality at scale. As manufacturers shift toward plant-based formulations, mixing equipment must handle low-viscosity liquids with suspended solids while preventing separation during storage and filling. Fristam’s inline colloid mixing technology provides the controlled shear and process reliability needed for these demanding applications.

Customer brief

A leading consumer goods manufacturer, known for established household brands across North America, partnered with a contract packager in Wisconsin to launch a new eco-friendly insecticide formulation. The product was based on cedar oil — a natural essential oil derived from cedar trees — selected for its effective pest-repellent properties and plant-based sustainability profile.

While the formulation performed well chemically, production challenges emerged during scale-up. The low-viscosity liquid contained suspended solids that separated during holding and filling. This caused visible inconsistency in the packaged product and risked compromising both appearance and performance, creating a barrier to commercial launch.

Previously unsuccessful methods

The manufacturer had previously trialled a competing colloid mill for similar emulsification tasks. However, the system proved unsuitable for production use due to:

  • Complex and time-consuming cleaning procedures
  • Limited operational flexibility
  • Requirement for partial disassembly to adjust shear settings

These limitations increased downtime and reduced line efficiency, prompting the search for a more adaptable, hygienic, and production-friendly mixing solution.

Previously unsuccessful methods

Fristam’s solution

Fristam recommended an on-site production trial using the Fristam FCM Colloid Mixer, an advanced inline mixing system designed to handle difficult emulsions and formulations containing suspended solids.

The objective of the trial was to evaluate emulsification performance, process stability, operational flexibility, and the potential to simplify the overall production line layout.

Trial set-up

1. Initial feed pump configuration
The formulation was initially supplied to the FCM using a conventional rubber lobe feed pump. A secondary pump was used downstream to maintain process flow. Multiple operating speeds and rotor-stator settings were tested to establish baseline shear performance.

2. Self-suction capability evaluation
During operation, inlet pressure readings indicated vacuum at the mixer inlet, suggesting that the FCM was capable of drawing product directly from the supply tote. The feed pump was removed to validate this capability.

3. Direct suction processing
With the feed pump removed, the FCM maintained continuous, stable flow above 40 gallons per minute (150 litres per minute). Product samples were collected and compared against the original pump-fed configuration.

4. Laboratory verification
Processed samples were sent for laboratory analysis to confirm emulsification quality, suspended solid distribution, and long-term stability under storage conditions.

Fristam’s solution

A successful outcome with the Fristam FCM

The Fristam FCM delivered consistent, stable emulsification while completely eliminating ingredient separation during production and storage. Laboratory testing confirmed uniform dispersion of suspended solids, ensuring consistent product appearance and active ingredient performance.

By operating reliably in direct suction mode, the FCM removed the need for a separate feed pump while maintaining production flow rates above 150 litres per minute. This simplified the production layout, reduced equipment complexity, and lowered overall energy demand.

Operational flexibility was significantly improved. Operators were able to adjust shear rates and process parameters quickly without disassembly, allowing fast optimisation for different formulations.

Following the successful trial, the contract packager committed to full-scale deployment of the Fristam FCM and is now evaluating the addition of a second unit to support redundancy and future production expansion.

Do you have any questions so far?

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Process / Product quality benefits

Process / Product quality benefits

  • Consistent, repeatable emulsification with no phase separation
  • Uniform distribution of active ingredients and suspended solids
  • Stable product appearance during filling and storage
  • Adjustable shear control without mechanical disassembly
  • Fully CIP-capable design supporting hygienic production
Sustainability benefits

Sustainability benefits

  • Support for plant-based, environmentally friendly insecticide production
  • Reduced material waste through full ingredient utilisation
  • Lower energy consumption by eliminating auxiliary pumping equipment
  • Reduced cleaning water usage through efficient CIP integration
Financial benefits

Financial benefits

  • Elimination of a dedicated feed pump, reducing capital equipment requirements
  • Simplified line layout lowering maintenance and service costs
  • Reduced cleaning time and labour requirements
  • Faster line changeovers improving overall equipment utilisation
  • Indicative equipment savings of approximately $4,000 / €3,700 through feed pump removal
Other benefits

Other benefits

  • Compact footprint suitable for existing production environments
  • Operator-friendly parameter adjustment
  • Reliable high-flow operation without feed assistance
  • Improved process stability for contract packaging operations

Similar applications

The Fristam FCM Colloid Mixer is ideally suited for the following similar applications:

  • Natural and botanical formulations
  • essential oil dispersions
  • nano-emulsions for nutraceuticals and personal care
  • flavour emulsions, CBD oil mixtures
  • food sauces and condiments
  • dairy emulsions and homogenised beverages
  • water-in-oil cosmetic emulsions
  • cleaning product blends with suspended solids
  • veterinary and agricultural spray formulations

In addition to mixing & blending technology – check out Fristam’s full range of pumping technologies suitable for the chemical industry.

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